Whatever the reason, I have learned several things.
One: There is quite a lot of sludge left (which the recipe says can be used for a second batch of ink), reducing the yield of actual liquid to write with quite a bit... to about half, actually, in my case.
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Sludge left, ink right...
Two: It's a fairly viscous ink. That is a nice thing as it makes using the ink on fabric a bit easier than when it's more liquid - though with a bit of practice, that is also no problem.
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The ink test on fabric...
So that would make this ink nicely suitable for use as embroidery pre-drawing... if there were not number
Three: It's too oxidised, and that means there are too many free-floating ink particles in the liquid. Which means that though it will not wash out, it will bleed - and this, in turn, means I will look for (and try) a different recipe, and see if that works better.
The ink I have now is still a nice ink, though not for pre-drawing. It does give a lovely black on paper or parchment, though, and that usually does not get washed... so if someone needs some writing ink, let me know!